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Get DetailsCup is ready for testing. Thermo Scientific Niton XL2 Analyzer User’s Guide... Page 72: Preparing Mining Samples About 4-6 g of dry pulverized sample is calcinated in an alumina or platinum crucible in a muffle furnace at 1000C for 1 hour. b.
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Get DetailsFeb 16, 2022 After washed alternately with deionized water and absolute ethanol, the white precipitate was removed by centrifuge and added into sodium hydroxide solution (0.1 M) for 1 hour. Finally, the sample was annealed in a muffle furnace at 400 C for 2 hours to get powder for later use. 2.2. Synthesize TiO 2 with dominant {101} facets (T-101)
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Get DetailsMar 08, 2022 Thirdly, the dried samples with the porcelain crucibles were put into a muffle furnace together and burned at 380 C for 1 h, and then crucibles were removed into a desiccator rapidly when the furnace fell to 100–150 C. Then the porcelain crucibles were weighed (m 3) until dropping to room temperature and calculated the organic matter ...
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Get DetailsThe precipitate was collected on Whatman 0.2-μm glass filter paper, rinsed several times with deionized water and ethyl alcohol, and subsequently dried at 70 C for 12 h under vacuum condition. The dried powder was heated to 300 C at a ramp rate of 1 C min −1 under ambient air atmosphere in a muffle furnace and then then kept for 300 min.
Get DetailsThen, 400 mg of MCM-41 MS was added to the above solution with vigorous stirring at 80 C for 1 h. The obtained mixture was dried at 80 C overnight. After grinding, the mixture was heated to 550 C in a muffle furnace at a heating rate of 5 C/min in air.
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